2-Chloro-N-(2,6-dimethylphenyl)acetamide synthesis
- Product Name:2-Chloro-N-(2,6-dimethylphenyl)acetamide
- CAS Number:1131-01-7
- Molecular formula:C10H12ClNO
- Molecular Weight:197.66
87-62-7
454 suppliers
$10.00/5 g
1131-01-7
346 suppliers
$7.00/5g
Yield:1131-01-7 89%
Steps:
289.A 2-chloro-N-(2,6-dimethylphenyl)acetamide
EXAMPLE 289A 2-chloro-N-(2,6-dimethylphenyl)acetamide The procedure described in Example 22A was followed, substituting 2,6-dimethylphenylamine for 3,4,5-trimethoxyaniline to provide the title compound (7.21 g, 89%) 1H NMR (300 MHz, CDCl3) δ 2.25 (s, 6H), 4.26 (s, 2H), 6.65 (t, J=7.46 Hz, 1H, 6.95 (d, J=7.46 Hz, 2H), 7.84 (s, 3H); MS (ESI) m/e 198 (M+H)+.
References:
Bhatia, Pramila A.;Daanen, Jerome F.;Hakeem, Ahmed A.;Kolasa, Teodozyj;Matulenko, Mark A.;Mortell, Kathleen H.;Patel, Meena V.;Stewart, Andrew O.;Wang, Xueqing;Xia, Zhiren;Zhang, Henry Q. US2004/29887, 2004, A1
144-55-8
1294 suppliers
$10.00/25g
79-04-9
347 suppliers
$12.00/5g
87-62-7
454 suppliers
$10.00/5 g
1131-01-7
346 suppliers
$7.00/5g