Ethyl 2-cyano-3,3-diphenylacrylate synthesis
- Product Name:Ethyl 2-cyano-3,3-diphenylacrylate
- CAS Number:5232-99-5
- Molecular formula:C18H15NO2
- Molecular Weight:277.32
119-61-9
805 suppliers
$5.00/10g
105-56-6
454 suppliers
$10.00/5ml
5232-99-5
299 suppliers
$6.00/10g
Yield:5232-99-5 94.1%
Reaction Conditions:
with ammonium acetate;pyrographite in n-heptane for 15 h;Ionic liquid;Reflux;
Steps:
4-7 Example 6 Preparation of ethyl 2-cyano-3,3-diphenylacrylate
According to the scheme in Example 4,Where ammonium acetate feeding scheme,Add 10g for the first time, after 1h of reaction,Then add 1.5g every half hour, the total reaction time is about 15h,The rest is unchanged, and finally the ethyl 2-cyano-3,3-diphenylacrylate is 117.1g,The yield was 94.1%, and the HPLC purity was 99.3%.
References:
Li'anlong Kerun (Zhejiang) New Materials Co., Ltd.;Tianjin Li'anlong New Materials Co., Ltd.;Zheng Hongchao;Zhang Junhua;Li Ying;Jiang Tingting;He Huolei;Sun Chunguang;Li Haiping CN110981752, 2020, A Location in patent:Paragraph 0093-0094; 0099-0104
1013-88-3
388 suppliers
$10.00/5g
105-56-6
454 suppliers
$10.00/5ml
5232-99-5
299 suppliers
$6.00/10g
119-61-9
805 suppliers
$5.00/10g
631-61-8
810 suppliers
$11.19/100G
64-19-7
1586 suppliers
$10.00/25ML
105-56-6
454 suppliers
$10.00/5ml
71-43-2
718 suppliers
$11.19/25ML
5232-99-5
299 suppliers
$6.00/10g