N-Pyridin-2-ylmethyl-formamide synthesis
- Product Name:N-Pyridin-2-ylmethyl-formamide
- CAS Number:56625-03-7
- Molecular formula:C7H8N2O
- Molecular Weight:136.15
Yield:56625-03-7 100%
Reaction Conditions:
for 1.5 h;Reflux;
Steps:
14 4.1.14. N-(pyridin-2-ylmethyl)formamide (11a).
4.1.14. N-(pyridin-2-ylmethyl)formamide (11a). A solution of 1-(pyridin-2-yl)methanamine (10a, 10.8?g, 10.3?mmol) and ethyl formate was heated under reflux with magnetic stirring for 1.5?h. After completion of the reaction, the resulting mixture was evaporated to give the final product 11a as yellow oil, 13.5?g (quant.). [14].
References:
Bátori, Sándor;Csányi, Dorottya;Takács, Daniella;Egyed, Orsolya;Riedl, Zsuzsanna;Hajós, Gy?rgy [Tetrahedron,2019,vol. 75,# 2,p. 180 - 185]
3731-51-9
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