3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97
- CAS No.
- 19962-04-0
- Chemical Name:
- 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97
- Synonyms
- Neostigmine bromide Impurity 4;Neostigmine bromide Impurity L;3-Aminophenyl dimethylcarbamate;3-aminophenyl N,N-dimethylcarbamate;Cyclobutanecarboxylicacid,3,5-difluoro-;3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97;N,N-Dimethylcarbamic acid 3-aminophenyl ester;Carbamic acid, N,N-dimethyl-, 3-aminophenyl ester
- CBNumber:
- CB8506775
- Molecular Formula:
- C9H12N2O2
- Molecular Weight:
- 180.2
- MDL Number:
- MFCD00052699
- MOL File:
- 19962-04-0.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 3-Aminophenyldimethylcarbamate | 2429CA | 100mg | $153 |
| 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE 95.00% | CHM0023310 | 250MG | $598.97 |
| 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE 95.00% | CHM0023310 | 1G | $733.96 |
| 3-Aminophenyldimethylcarbamate 97% | A119757 | 5g | $784 |
| 3-Aminophenyldimethylcarbamate 95%-98% | 61-3026 | 0.25g | $882 |
| More product size | |||
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 price More Price(10)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| AK Scientific | 2429CA | 3-Aminophenyldimethylcarbamate | 19962-04-0 | 100mg | $153 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | CHM0023310 | 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE 95.00% | 19962-04-0 | 250MG | $598.97 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | CHM0023310 | 3-AMINOPHENYL N,N-DIMETHYLCARBAMATE 95.00% | 19962-04-0 | 1G | $733.96 | 2021-12-16 | Buy |
| Ambeed | A119757 | 3-Aminophenyldimethylcarbamate 97% | 19962-04-0 | 5g | $784 | 2021-12-16 | Buy |
| Abosyn | 61-3026 | 3-Aminophenyldimethylcarbamate 95%-98% | 19962-04-0 | 0.25g | $882 | 2021-12-16 | Buy |
3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 Chemical Properties,Uses,Production
Synthesis
7244-70-4
591-27-5
19962-04-0
GENERAL STEPS: To a dry 500 mL four-necked round-bottomed flask were added dimethyl sulfoxide (DMSO, 100 mL), 3-aminophenol (67.5 g) and sodium hydroxide (NaOH, 24.7 g). The reaction mixture was heated to 75-80 °C and maintained at this temperature for 4 hours. Subsequently, 4-nitrophenyl-N,N-dimethylcarbamate (100 g) and DMSO (100 mL) were added in batches at the same temperature. The reaction temperature was raised to 110-120 °C and the reaction was continued for 2 hours. The progress of the reaction was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction was quenched with 1% sodium hydroxide solution (1500 mL). Extraction was carried out with methylene chloride (MDC), the organic layer was separated, washed with water, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was recrystallized with toluene to obtain pure 3-aminophenyl dimethylcarbamate. Yield: 62 g (72.2% yield). Melting point: 83-85°C (literature value: 80-86°C, FR 1498834).
References
[1] Patent: WO2017/175238, 2017, A1. Location in patent: Page/Page column 31
3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97 Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Coresyn Pharmatech Co., Ltd. | +86-571-86626709 +86-18157142896 | cbc@coresyn.com | China | 9984 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 52923 | 58 | |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131957 | 58 |
| Chemwill Asia Co.,Ltd. | 86-21-51086038 | chemwill_asia@126.com | CHINA | 23912 | 58 |
| Adamas Reagent, Ltd. | 400-6009262 16621234537 | chenyj@titansci.com | China | 14101 | 59 |
| Shanghai Raise Chemical Technology Co.,Ltd | 15026594951 | rs@raise-chem.com | China | 4454 | 55 |
| Shanghai Raise Chemical Technology Co.,Ltd | +86-021-50935922 | China | 7865 | 55 | |
| ChemStrong Scientific Co.,Ltd | 0755-0755-66853366 13670046396 | sales@chem-strong.com | China | 18333 | 56 |
| Shanghai Kewel Chemical Co., Ltd. | 021-64609169 18901607656 | greensnown@163.com | China | 9906 | 50 |
19962-04-0(3-AMINOPHENYL N,N-DIMETHYLCARBAMATE, 97)Related Search:
1of4
