ChemicalBook CAS DataBase List 2-Pyridinylcarbamicacidethylester

2-Pyridinylcarbamicacidethylester synthesis

13synthesis methods

Product Name:2-Pyridinylcarbamicacidethylester
CAS Number:5255-67-4
Molecular formula:C8H10N2O2
Molecular Weight:166.18

504-29-0
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$5.00/5G

64-17-5 Synthesis

64-17-5
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24424-99-5 Synthesis

24424-99-5
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$13.50/25G

5255-67-4
21 suppliers
$278.00/5g

Yield:5255-67-4 99%

Reaction Conditions:

at 0 - 20; for 4 h;Inert atmosphere;

Steps:

General Procedure for Preparation of Carbamates (2)

General procedure: All the reactions were carried out on 10mmol scale. 2-Aminopyridine was dissolved in appropriate alcohol (3times) and cooled to 0oC. To this solution Boc anhydride(1.2Eq) was added and reaction mixture was allowed to coolto room temperature. Reaction mixture was stirred at thesame temperature for 4hr. Half volume of the alcohol wasremoved on rotavapor. Solid separated was collected by filtration.

References:

Shewalkar, Mukesh P.;Rao, Ramakrishna R.;Reddy, Veerbhadra;Darandale, Sunil N.;Shinde, Devanand B. [Letters in Organic Chemistry,2013,vol. 10,# 1,p. 60 - 64]

504-29-0
537 suppliers
$5.00/5G