Hexafluoroisopropyl methyl ether synthesis
- Product Name:Hexafluoroisopropyl methyl ether
- CAS Number:13171-18-1
- Molecular formula:C4H4F6O
- Molecular Weight:182.06
74-87-3
222 suppliers
$18.50/48622
920-66-1
651 suppliers
$6.00/10g
13171-18-1
212 suppliers
$48.00/5g
Yield:13171-18-1 192 g
Reaction Conditions:
with anhydrous sodium carbonate in (methylsulfinyl)methane at 80 - 90; for 12 h;
Steps:
3 Example 3
185g of methyl chloride, 300g of sodium carbonate and 3.5L of dimethyl sulfoxide were added to the reactor, 168g of hexafluoroisopropanol was added after stirring at room temperature for three hours, the temperature was controlled at 80-90°C, and the reaction was stirred for 12 hours. Distilled at ~110°C at atmospheric pressure to obtain fractions, which were washed three times with water to obtain 192 g of chloromethyl-2,2,2-trifluoro-1-(trifluoromethyl)ethyl ether with a GC purity of 97.65%.
References:
CN114671742,2022,A Location in patent:Paragraph 0036-0037
67-56-1
790 suppliers
$9.00/25ml
920-66-1
651 suppliers
$6.00/10g
13171-18-1
212 suppliers
$48.00/5g
920-66-1
651 suppliers
$6.00/10g
77-78-1
319 suppliers
$22.00/25g
13171-18-1
212 suppliers
$48.00/5g
124-41-4
731 suppliers
$12.00/25g
67674-48-0
92 suppliers
$11.19/5G
13171-18-1
212 suppliers
$48.00/5g
37021-26-4
0 suppliers
inquiry
13171-18-1
212 suppliers
$48.00/5g